熱分析應(yīng)用手冊：彈性體

應(yīng)用一覽表 Applications List!
1.熱分析概論IntroductionTo Thermal Analysis
1.1 差示掃描量熱法Differential Scanning Calorimetry(DSC)
1.1.1 常規(guī)DSC Conventional DSC
1.1.2 溫度調(diào)制DSC Temperature－modulated DSC
1.2 熱重分析了hermo Gravimetric Analysis(TGA)
1.3 熱機(jī)械分析了hermo Mechanical Analysis(TMA)
1.4 動(dòng)態(tài)熱機(jī)械分析Dynamic Mechanical Analysis(DMA)
1.5 與TGA的同步測量SimuLTaneous Measurements with Tga
1.5.1 同步DSC和差熱分析Simultaneous DSC and differential thermal analysis(DTA，SDTA
1.5.2 逸出氣體分析Evolved gas analysis(EGA)
1.5.2.1 TGA－MS
1.5.2.2 TGA－FTIR
2.彈性體的結(jié)構(gòu)、性能和應(yīng)用Structure.Properties and Applications of Elastomers
2.1 聚合物的結(jié)構(gòu)Structure of Polymers
2.1.1 大分子中單體的排列Arrangement of monomers in a macromolecule
2.1.2 大分子的結(jié)構(gòu)Structure of macromolecules
2.2 聚合物的物理結(jié)構(gòu)Physical Structure of Polymers
2.3 聚合物材料的分類Classification of Polymeric Materials
2.4 彈性體產(chǎn)品Elastomeric Products
2.4.1 聚合物的交聯(lián)Cross－linking of polymers
2.4.2 彈性體的生產(chǎn)Manufacture of elastomers
2.4.3 彈性體的組成Composition of elastomers
2.5 彈性體的分類Classfication of Elastomers
2.6 彈性體實(shí)例Examples of Elastomers
2.7 彈性體分析Analysis of Elastomers
2.7.1 熱效應(yīng)了hermal effects
2.7.2 應(yīng)用概述Application overview
2.7.3 彈性體分析標(biāo)準(zhǔn)方法匯總Summary of standard methods for elastomer analysis45
3.彈性體的基本熱效應(yīng)BasicThermal Effects of Elastomers
3.1 DSC測試效應(yīng)Measurement Effects with DSC
3.1.1 玻璃化轉(zhuǎn)變的計(jì)算方法Evaluation of glass transitions
3.1.2 結(jié)晶和熔融Crystallization and melting
3.1.3 硫化反應(yīng)Vulcanization reaction
3.1.4 借助ADSC用于曲線解析了he use of ADSC to aid curve intcrprctati.n93
3.2 效應(yīng)的TGA測量Measurement Effects with TGA
3.2.1 組分分析的基本原理Basic principles of compositional analysis
3.2.2 實(shí)驗(yàn)條件的影響Influence of experimental conditions
3.2.3 計(jì)算方法Evaluation possibilities
3.3 TMA測量TMA Measurements
3.3.1 膨脹系數(shù)的測量Measurement of the expansion coefficient
3.4 DMA實(shí)驗(yàn)DMA Experiments
3.4.1 復(fù)合力學(xué)性能The complex mechanical properties
3.4.2 DMA曲線的計(jì)算和表示Evaluation and presentation of DMA curves
3.4.3 玻璃化轉(zhuǎn)變和松弛Glass transition and relaxation
4.熱分析的應(yīng)用Applications.f Thermal Analysis
4.1 橡膠的分析Analysis of Rubber
4.1.1 不同種類橡膠的TGA分析TGA analysis of different types of rubber
4.1.2 玻璃化轉(zhuǎn)變Glass transition
4.1.3 結(jié)晶和熔融Crystallization and melting
4.1.4 DSC和DMA測量的比較Comparison of DSC and DMA measurements
4.2 硫化Vulcanization
4.2.1 硫化反應(yīng)Vulcanization reactions
4.2.2 SBR硫化度對其熱分析結(jié)果的影響Influence of the degree of vulcanization.n thc resultS of SBR
4.2.3 硫化和未硫化硅橡膠的DSC比較Comparison of vulcanized and unvulcanized silic.nc elastomers by DSC
4.3 碳黑的影響The Influence of Carbon Black
4.3.1 碳黑的分析Analysis of carbon black
4.3.2 測定碳黑對彈性體影響的DSC測量DSC measurements tO determine the effect.f carb.n black on elastomers
4.3.3 彈性體中碳黑的TGA分析Analysis of carbon black in elastomers byTGA
4.3.4 含碳黑填料彈性體的TMA測量TMA of elastomers with carbon black fillers
4.3.5 碳黑填充彈性體的DMA測量Measurement of carbon black filled elastomers by DMA
4.4 以單一聚合物為基礎(chǔ)的彈性體的實(shí)驗(yàn)Experiments on Elastomers Based on a Single Type Polymer
4.4.1 TGA分析TGA Analysis
4.4.2 彈性體的氣體分析鑒別Identification of elastomers by means of gas analysis
4.4.3 DSC測量DSC Measurements
4.4.4 低分子量成分的熔融和結(jié)晶Melting and crystallization of low molecular weight components
4.5 含若干個(gè)聚合物成分的彈性體Elastomers with Several Polymer Components
4.5.1 TGA測量TGA Measurements
4.5.2 彈性體組分的TGA／FTIR鑒定Identification of the polymer constituents byTGA－FTIR
4.5.3 DSC測量DSC measurements
4.5.4 復(fù)雜彈性體的分析實(shí)例Example of a complex elastomer analysis
4.5.5 DMA測量DMA measurements
4.6 彈性體中油和增塑劑的分析Analysis of Oils And Plasticizers In Elastomers
4.6.1 油含量的TGA測定Determination of the oil content by TGA
4.6.2 增塑劑對玻璃化轉(zhuǎn)變的影響Influence of plasticizers on the glass transition
4.7 添加劑和助劑的分析Analysis of Additives and Auxiliary Agents
4.7.1 阻燃劑Flame retardants
4.7.2 增塑劑Plasticizers
4.8 彈性體的進(jìn)一步測量Further Measurements of Elastomers
4.8.1 TMA測量TMA measurements
4.8.2 DSC測量DSC measurements
5.結(jié)果的總結(jié)Summary of Results
參考文獻(xiàn)Literature