第1章 逸出氣體分析簡(jiǎn)介 Introduction to Evolved Gas Analysis(1) 第2章 熱重-質(zhì)譜聯(lián)用技術(shù)TGA-MS(6) 2.1質(zhì)譜的原理 Principles of MS(6) 2.2TGA-MS 測(cè)量系統(tǒng) The TGA-MS System(8) 2.3測(cè)量模式 Measurement Modes(9) 2.4結(jié)果解釋 Interpretation of Results(11) 2.5典型的碎片化模式 Typical Fragmentation Patterns(15) 2.6結(jié)果表述 Presentation of Results(16) 第3章 熱重-紅外光譜聯(lián)用技術(shù)TGA-FTIR (17) 3.1FTIR的原理 Principles of FTIR(17) 3.2TGA-FTIR系統(tǒng) The TGA-FTIR System(21) 3.3曲線表示 Presentation of Results(22) 3.4解析方法 Interpretation Procedure(24) 3.5光譜的解析 Interpretation of Spectra(26) 3.6特征吸收頻率 Characteristic Absorption Frequencies(27) 3.7結(jié)果表述 Presentation of Results(29) 第4章 熱重分析-氣相色譜/質(zhì)譜聯(lián)用技術(shù)TGA-GC/MS (30) 4.1GC的原理 Principles of GC(30) 4.2TGA-GC/MS系統(tǒng) The TGA-GC/MS System(35) 4.3測(cè)量可行性 Measurement Possibilities(36) 4.4測(cè)量結(jié)果 Results(39) 第5章 熱重分析-微型氣相色譜/質(zhì)譜聯(lián)用技術(shù)TGA-Micro GC/MS (41) 5.1微型氣相色譜儀的原理 Principles of Micro GC(41) 5.2TGA-Micro GC和TGA-Micro GC/MS系統(tǒng) TGA-Micro GC and TGA-Micro GC/MS Systems(44) 5.3實(shí)驗(yàn)結(jié)果 Results(45) 第6章 應(yīng)用簡(jiǎn)介 Introduction to the Applications (46) 第7章應(yīng)用介紹 Applications List (49) 7.1通過(guò)TGA-MS、TGA-FTIR和TGA-MicroGC研究一水合草酸鈣的分解機(jī)理 Decomposition of Calcium Oxalate Monohydrate (Tutorial) by TGA-MS, TGA-FTIR and TGA-Micro GC(55) 7.2通過(guò)TGA-MS和TGA-FTIR研究五水合硫酸銅的分解機(jī)理 Decomposition of Copper Sulfate Pentahydrate (Tutorial) by TGA-MS and TGA-FTIR(57) 7.3實(shí)驗(yàn)條件對(duì)MS靈敏度的影響分析 Influence of Experimental Conditions on MS Sensitivity(59) 7.4通過(guò)TGA-MS和TGA-GC/MS多次進(jìn)樣法研究乙酰水楊酸的分解 Decomposition of Acetylsalicylic Acid by TGA-MS and TGA-GC/MS Multi-injection(65) 7.5通過(guò)TGA-FTIR研究BHET的熱降解 Thermal Degradation of BHET by TGA-FTIR(67) 7.6通過(guò)TGA-FTIR研究工業(yè)月桂醇的分解 Decomposition of Technical Lauryl Alcohol by TGA-FTIR(70) 7.7通過(guò)TGA-MS檢測(cè)藥物中的殘留溶劑 Detection of Residual Solvents in a Pharmaceutical Substance by TGA-MS(72) 7.8通過(guò)TGA-MS研究填充有機(jī)物的沸石的解吸附 Desorption of a Zeolite Filled with Organic Matter by TGA-MS(73) 7.9通過(guò)TGA-MS研究PVC粉末的熱裂解 Pyrolysis of PVC Powder by TGA-MS(76) 7.10通過(guò)TGA-FTIR研究氟化電纜線 Investigation of Fluorinated Cable Wires by TGA-FTIR(78) 7.11通過(guò)TGA-MS檢測(cè)橡膠樣品中的水楊酸甲酯 Detection of Methyl Salicylate in a Rubber Sample by TGA-MS(80) 7.12通過(guò)TGA-FTIR研究有機(jī)硅聚合物的降解 Degradation of a Silicone Polymer by TGA-FTIR(81) 7.13通過(guò)TGA-MS和TGA-FTIR研究氨基樹(shù)脂的固化和分解 Curing and Decomposition of an Amino Resin by TGA-MS and TGA-FTIR(83) 7.14通過(guò)TGA-FTIR和DSC研究熱轉(zhuǎn)變和分解以鑒別BR和NR橡膠 Identification of BR and NR Rubbers. Study of Thermal Transitions and Decomposition by TGA-FTIR and DSC(85) 7.15通過(guò)TMA-MS研究印刷電路板的分層 Delamination of Printed Circuit Boards by TMA-MS(88) 7.16通過(guò)TMA-MS研究用于封裝發(fā)泡劑的聚合物的膨脹和分解 Expansion and Decomposition of a Polymer Used To Encapsulate a Blowing Agent by TMA-MS(89) 7.17通過(guò)TGA-MS測(cè)定離子液體中的水分含量 Determination of the Water Content of an Ionic Liquid by TGA-MS(91) 7.18通過(guò)TGA-FTIR研究熱裂解并闡明阻燃機(jī)理 From the Investigation of Pyrolysis to the Elucidation of Fire Retardancy Mechanisms by TGA-FTIR(93) 7.19通過(guò)TGA-MS和DSC研究高熔點(diǎn)陶瓷 High Melting Ceramics by TGA-MS and DSC(97) 7.20通過(guò)TGA-MS和顯微DSC研究唑來(lái)膦酸水合物的熱行為 Thermal Behavior of Zoledronic Acid Hydrate by TGA-MS and DSC-Microscopy(100) 7.21通過(guò)TGA-MS定量分析鈷粉中的氧化鈷 Quantification of Cobalt Oxide in a Coated Cobalt Powder by TGA-MS(103) 7.22通過(guò)TGA-GC/MS和TGA-Micro GC/MS研究聚酰胺66的分解產(chǎn)物 Investigation of Evolved Decomposition Products of Polyamide66 by TGA-GC/MS and TGA-Micro GC/MS(104) 7.23通過(guò)TGA-GC/MS、DSC和DMA鑒定多組分熱塑性樹(shù)脂 Identification of Multi-Component Thermoplastics by TGA-GC/MS, DSC and DMA(107) 7.24通過(guò)TGA-GC/MS、DSC、DMA和ATR研究橡膠的變形原因 Deformulation of a Rubber by TGA-GC/MS, DSC, DMA and ATR(113) 7.25通過(guò)TGA-GC/MS-FTIR測(cè)定聚丙烯材料有無(wú)磷酸銨阻燃劑的性質(zhì) Polypropylene with and without Ammonium Phosphate Flame Retardant by TGA-GC/MS-FTIR(120) 7.26通過(guò)TGA-GC/MS對(duì)EPDM橡膠進(jìn)行熱氧化研究 Thermal Oxidation of EPDM Rubber by TGA-GC/MS(125) 7.27通過(guò)TGA-MS和TGA-GC/MS定量分析涂料中的二甲基甲酰胺（DMF） Quantification of Dimethylformamide in Coatings by TGA-MS and TGA-GC/MS(129) 7.28TGA-GC/MS定量測(cè)定天然橡膠中低含量的丁苯橡膠 Quantification of a Low Content of Styrene-Butadiene Rubber in Natural Rubber by TGA-GC/MS(134) 7.29通過(guò)TGA-Micro GC/MS技術(shù)分析酚醛樹(shù)脂的分解產(chǎn)物 Evolved Decomposition Products of a Phenol-Formaldehyde Resin by TGA-Micro GC/MS(137) 7.30通過(guò)TGA-Micro GC/MS技術(shù)定量分析焦炭樣品中的二氧化碳 Quantification of Carbon Dioxide in a Coke Sample by TGA-Micro GC/MS(140) 7.31TGA-Micro GC/MS、TMA和DSC用于鈦酸鋇的合成和表征 Synthesis and Characterization of Barium Titanate by TGA-Micro GC/MS, TMA and DSC(142) 7.32用TGA-Micro GC/MS和Karl Fischer滴定儀測(cè)定熱塑性塑料中的水含量 Determination of Water Content in a Thermoplastic by TGA-Micro GC/MS and Karl Fischer titrator(147) 7.33通過(guò)TGA-GC/MS和TGA-Micro GC/MS研究生物質(zhì)樣品 Study of a Biomass Sample by TGA-GC/MS and TGA-Micro GC/MS(151) 7.34通過(guò) TGA-GC/MS和TGA-Micro GC/MS分析由褐煤釋放出的氣體 Gases Evolved from Lignite by TGA-GC/MS and TGA-Micro GC/MS(157) 參考書(shū)目 Literature(164) 縮寫(xiě)和首字母縮寫(xiě)詞 Abbreviations and Acronyms(165)
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