部分 緒論 、物理化學實驗的目的和要求 二、物理化學實驗的安全知識 三、物理化學實驗的設計思想和方法 四、誤差理論和有效數(shù)字 五、實驗數(shù)據(jù)的表示法 art One Introduction Objective and requirement Physical chemistry laboratory safety Rules and methods for designing of the physical chemistry experiment Error theory and significant figures Data reporting 第二部分 實驗 art Two Experiments 實驗一 燃燒熱的測定 Experiment 1 Determination of Heats of Combustion 實驗二 溶解熱曲線的測定 Experiment 2 Determination of Heats of Solution Curve 實驗三 凝固點降低法測定摩爾質量 Experiment 3 Determination of Molar Mass by Freezing Point Depression 實驗四 凝固點降低法測定氫化納注射液的滲透壓 Experiment 4 Determination of Osmotic Pressure of Sodium Chloride Injection by Freezing Point Depression 實驗五 靜態(tài)法測定液體飽和蒸氣壓 Experiment 5 Saturated Vapor Pressure of Pure Liquids by Static Method 實驗六 反應平衡常數(shù)及分配系數(shù)的測定 Experiment 6 Determination of Equilibrium Constant of Reaction and Partition Coefficient 實驗七 二組分部分§溶雙液系統(tǒng)目國的繪制 Experiment 7 Drawing of Phase Diagram for a Partially Miscible Binary Liquid System 實驗八 §溶雙液系統(tǒng)平衡目國的繪制 Experiment 8 Drawing of Phase Diagram for a Miscible Binary Liquid System 實驗九 二組分簡單低共熔系統(tǒng)目國的繪制 Experiment 9 Drawing of Phase Diagram for a Binary utectic System 76 實驗十 三組分液-液系統(tǒng)目國的繪制 78 Experiment 10 Drawing of Phase Diagram for a Ternary Liquid System 實驗十一 電解質水溶液電導的測定及應用 Experiment 11 Measurement and Application of lectrolyte Solution Conductance 實驗十二 電動勢法測溶液 pH 相反應熱力學函數(shù) xperiment 12 Determination of pH of Solutions and Thermodynamic Functions by lectromotive Force Measurements 實驗十三 旋光法測定康糖轉化反應的速率常數(shù) Experiment 13 Determination of Rate Constant for the Conversion of Sucrose by Polarimetric Method 實驗十四 乙酸乙醋皂化反應速率常數(shù)及活化能的測定 Experiment 14 Determination of Rate Constant and Activation nergy for the Saponification of thyl Acetate by Conductometric Method 實驗十五 腆化擁與過氧化氫反應的速率常數(shù)及活化能的測定 Experiment 15 Determination of Rate Constant and Activation nergy for Reaction between Potassium Iodide and Hydrogen Peroxide 實驗十六 丙酣漠化反應速率常數(shù)的測定 Experiment 16 Determination of Rate Constant for the Bromination of Acetone 實驗十七 氣泡壓力法測定液體表面張力 Experiment 17 Determination of the Solution Surface Tension by Bubble Pressure Method 實驗十八 固體在溶液中的眼附 Experiment 18 Adsorption of Solids in Solution 實驗十九 溶膠的制備及性質 Experiment 19 Preparation and Properties of Sols 實驗二十 黠度法測定大分子的平均目對分子質量 Experiment 20 Determination of Average Relative Molar Mass of the Macromolecule by Viscosity Method 實驗二十一 藥物多晶型的差熱分析(設計性實驗) Experiment 21 Thermal Analysis of Polymorphism Pharmaceuticals(Designing xperiment) 實驗二十二 藥物穩(wěn)定性及有效期測定(設計性實驗) Experiment 22 Determination of Drug Stability and Shelf Life(Designing experiment) 實驗二十三 載藥納米粒子的制備及表征(綜合設計性實驗) Experiment 23 Preparation and Characterization of Drug-loaded Nanoparticles(Comprehensive Designing xperiment) 實驗二十四 固體藥物常規(guī)理化常數(shù)的測定(綜合設計性實驗) Sxperiment 24 Determination of Physical and Chemical Constants of Solid Drugs(Comprehensive Designing xperiment) 實驗二十五 表面活性劑臨界膠束濃度的測定(綜合設計性試驗) Experiment 25 Determination of Critical Micelle Concentration for Surfactants(Comprehensive Designing xperiment) 實驗二十六 乳狀液的制備和性質(綜合設計性實驗) Experiment 26 Preparation and Properties of mulsion(Comprehensive Designing xperiment) 第三部分 實驗測試題 一、單選題 二、司口題 三、答案 art Three Experiment Test Questions Section One Multiple Choice Section Two Short Questions Section Three Answers 第四部分 附錄 Part Four Appendices 一、 常用物理化學實驗數(shù)據(jù)表(Common Data of xperimental Physical Chemistry) 二、 參考文獻(References)